Quick connect fitting block off made by the extremely talented J.D Guerard machining.
ALIS acquired from Andrew (http://rtftechnologies.org). CF flange, MHV feedthrough, and HV PSU are on order.
Ion source links: http://wiki.zeloof.xyz/index.php/Ion_Source
Abstract: Anode layer ion sources are one type of gridless (no acceleration or focusing grids/screens) closed-drift (electron and plasma movement is confined due to E x B force) ion sources and are therefore a simple way to make a confined ion/plasma stream. These sources commonly operate under partial vacuum in O2/N2/Ar environments. They have many applications, one of which is a high power directional plasma cleaning source which has many advantages over glow discharge or inductively/capacitively coupled plasmas. Their cylindrical geometry can be explained because it allows the E x B currents to converge and close in on themselves rather than being swept to one side in non-cylindrical designs. They are similar to inverted magnetrons and end-Hall ion thrusters in construction and in operation except they often do not require external neutralization for the ion beam.
Neutralizing electrons come from the from the surroundings and collisions of ions with the discharge channel walls because the anode is held at a higher potential than that of a hall effect source and they therefore operate in the self-sustained discharge area. Thus, some of the electrons from the cathode escape into the ion beam and neutralize the space charge on the ions. The extent of space charge neutralization can be related to the electric field strength and therefore the voltage applied to anode. These high voltages are typically in the 800v-2000v range and ALIS devices can operate up into the tens of millitorr down to the 1e-5 torr range at higher voltages. Continue reading Anode Layer Ion Source (RTFtechnologies)
You can see the opened specimen stage of my SEM in these pictures, notice the backscattered electron detector in the center of the coulumn in the second picture and the faraday cage on the right. The faraday cage is positively biased to attract secondary electrons to it and into the scintillator.
A 6mhz oscillator can was cut up with pliers and the top was removed to expose the quartz crystal. The output is AC coupled (high pass filtered) to the positive (+5v) rail so that a single coax cable can be used to connect this to the thickness monitor as the power is basically just a DC offset on the signal. If you buy a pack of crystals from somewhere like Lesker they will (depending on your thickness monitor) most likely require the usage of an external oscillator. Such a circuit can be made by a complimentary pair or NPN and PNP transistors and couple passive components. Thanks to Ben from Applied Science for the idea.
Abstract: The quartz microbalance is a quick way of monitoring thin film thicknesses in real time, a bare quartz crystal which oscillates at a known frequency is placed in the chamber near the substrate involved in deposition. As the film accumulates on the crystal, it gains mass and the resonant frequency is lowered. The cumulative frequency change is analyzed and interpreted as the rate of accumulation the rate is integrated into a total thickness. Note that accumulation rate is the proper term for deposition rate, as in many cases (sputtering) the actual deposition rate is higher but some atoms are resputtered off the substrate due to high energy molecules in the chamber, substrate temperature, etc. and the total film thickness can momentarily decrease. The net result of the deposition and resputtering is known as accumulation
+/- 0.1nm resolution!
My vacuum chamber which I am setting up for thermal evaporation has a large rectangular flange which has grooves for ISO style clamps and 2 locator pins. This flange may have been used for something like a load lock but as far as I could tell it is not a standard size so a custom block off plate was designed and machined from SS with grooves on the back for clamps, 2 pressed locator pins, and a viton o-ring. Mating surface was hand lapped to ensure good vacuum seal. Made by the extremely talented J.D Guerard machining company.