Miscellaneous Vacuum Chamber Upgrades – Microwave Plasma Interferometer

(Click on image to enlarge)

Photonic Nanostructes in Butterfly Wings – SEM Analysis

Nano-scale features on butterfly wing scales interact with specific wavelengths of visible light (photonic bandgap material) to produce bright colors as observed by the human eye. This structure, for example, removes certain wavelengths from the white light that hits it (mainly blue, 472nm) so that the color, when observed by the human eye, appears orange.

SEM Sample Preparation – DC Sputtering

Thin films of copper were prepared on non-conductive samples to be observed under the Electron Microscope. This process is called DC Diode Sputtering and took place at just below 100mTorr and 2000v @ 150watts.

materials-07-06377-g004-1024

This same setup can be used at lower powers to plasma clean or etch the top layer surface of the sample for better images under the SEM. Oxygen (and sometimes a small amount of Nitrogen) is usually a much more effective gas for this cleaning than Argon and leads to less unwanted sputtering as well.

Sputtering system v2 was made to support DC and RF sputtering so I can make dielectric coatings as well and it supports larger target and substrate samples. An insulator will be constructed to mount the target holder to the main chamber walls so that RF can be used more effectively.

(Click on image to enlarge)

SEM Demo

ICP Extraction and Plasma Cleaning

A simple Inductively Coupled Ion Source can be made by using a negative bias on an extractor cone or electrode to attract the positive ions and can later be focused into a beam with magnets. Such a source is suitable at high powers as a Deuteron source for an IEC fusor or for processes such as ion beam deposition or directional plasma cleaning. As seen in Patent #4,793,961, these architectures have been proven for exceptional use as hydrogen or deuterium ion sources.

The ICP coil is placed on a quartz tube mounted via a Kovar KF40 flange to the vacuum chamber and an antenna tuner (matching network) is used to couple the RF energy from 10 meter Ham radio transmitter to the coil. A Multi-cusp Magnetic assembly could be used as shown below to keep energetic electrons from being lost into the ion source walls, confine their motion, and reduce the occurrence of electron-ion recombination.

source

(Click on image to enlarge)

A high (low) negative voltage (usually between -400v and -2kv) is used on the extractor electrode. If this design was implemented in an IEC fusor, the extractor could be grounded because the fusor grid is held at a negative potential.

Fluorescence was observed in the quartz tube during these experiments due to electron bombardment. While the chamber was pumped down and MFCs setup, a DC copper sputtering environment was created for testing purposes as well as a controlled and isolated anode glow region of an incomplete glow discharge which forms a spherical region above the copper plate (anode) and could be used for uniform plasma cleaning.

Garage Electron Microscopy – First Images

A huge thanks to David Bono from the DMSE UGTL lab at MIT for training me in basic SEM operation during a recent college visit on MIT’s JEOL JSM-6400, which is very similar to my JSM-6300. Because of David Bono and Colin Marcus’s generosity I was able to get my SEM up and running.

thumb

Miscellaneous Vacuum Chamber Upgrades

Miscellaneous Upgrades – Vent Valve/TC Gauge CF Tee Construction, Gas Cylinder Holder Fabrication, and Ion Gauge Controller Analog Output Hack

My HP (Granville Phillips)  hot cathode ionization gauge controller (59822b) had provisions for an analog output however the optional connector was not installed on the back panel and the connection points on the main PCB of the controller did not show any voltage deflection proportional to pressure so I took the pressure output from one of the stages in the electrometer which happened to be one of the outputs of a quad opamp chip. This output is fed to a NI DAQ USB6009 and displayed in a LabView VI so that the pressure of the chamber while pumping down can be held constant when requested by PID feedback loop with one or more of the mass flow controllers.

A pressurized gas cylinder holder was designed and fabricated by Diversatech Manufacturing, INC (www.diversatech.com) for safer operation of my vacuum chamber when using gasses such as Oxygen, Nitrogen, or Argon for processes such as sputtering or plasma cleaning.

 

ICP Residual Gas Color Analysis

Due to different gasses pumping out of chambers at different rates (i.e. Hydrogen always has a low pumping speed) and air’s natural composition changing glow discharge colors can be observed while pumping down a vacuum chamber. This was an attempt to estimate the pressure of the chamber indirectly during a pump down by observing and analyzing the inductively coupled plasma color at constant RF voltage.

Ion Source Assisted Ignition of Inductively Coupled RF Plasma

Inductively coupled plasma (ICP) is a common method of ionizing the residual gas in a vacuum chamber. A RF source (commonly 13.56mhz) is connected to a coil (usually outside of the chamber) which induces currents in the nearby gas volume because of the time-varying magnetic fields.

I used a 10 meter (28mhz) 100 watt ham radio transmitter at 60mTorr with multiple coil designs to create an inductively coupled plasma. Even while minimizing the reflected power with a matching network (antenna tuner) the plasma was difficult to ignite. By briefly powering an anode layer ion source in proximity to the ICP coil I was able to ignite and sustain the ICP at lower power levels.

Once the ICP is sustained, the ALIS is powered off and the RF ICP remains on.

Paper written by Samuel Zeloof and Joshua Newstadt: A Brief Analysis of the Interactions Observed in Ion Clouds Created by Electric and Magnetic Fields From Multiple RF and DC Ion Sources

Anode Layer Ion Source Testing

 

Preliminary testing of the anode layer ion source (ALIS) from RTFtechnologies. I am waiting for MHV feedthroughs from Lesker and once they come I will be able to mount the ion source on a proper flange rather than having it rest on a KF adapter in the center of my chamber.

Tests were run at 50millitorr and between 800-1000v. Air plasma can been seen as low as 300v. Typical current at 1kv is 4ma. When the source is current limited, you can see a de-focusing effect as seen in the 2nd picture. This is because the ion source is not operating through the closed drift mechanism but is rather operating closer to a modified glow discharge under the influence of a local magnetic field.

Above pictures taken at much lower pressure and higher voltage (5e-4 torr and 4kv+)

ALIS mounted on 2.75″ CF flange via 10-32 standoff and electrical connection via MHV connector. As suggested and fabricated by J.D Guerard machining Co., a ditch was formed around the hole drilled for MHV feedthrough on the interior side of the flange which created a wall matching in thickness to the MHV connector feedthrough to facilitate with fusing. This can be seen in the first picture. When welded, the two surfaces of identical thickness are fused together easier, with lower current (this weld was done at only 20amps), and with consequently with no warping of the entire flange because of the localized heat.

Using the anode layer ion source as a crude ion pump (far from ideal conditions,  stainless steel chamber walls do not have high getter/sputter capacity)

Ion source power up sweep 400v – 4000v